Paul HagerPhD student

My project aims to implement a high-throughput method for the structural
characterization of metal organic frameworks (MOFs) by electron diffraction
(ED). Compared to X-ray diffraction - the established method for structure elu-
cidation of crystalline materials - ED exhibits a lower demand on sample size
and quality. By omitting the need for extensive sample preparation, it is tar-
geted to drastically speed up the development of novel MOF materials. In this
approach, a variety of different new phases can be synthesized in a single batch
(eg. by ball milling). The obtained compounds are then surveyed for phases
with the desired structural characteristics in a fully automated process. This is
possible without the need of tweaking the synthesis in the initial stage of the
development process. After the identification of a few promising structures in
a plethora of potential candidates, experimental resources for the optimization
of the synthesis for the desired compounds, can be utilized in a targeted man-
ner. By demonstrating the effectiveness of this approach, the project strives to
promote sustainable synthesis methods and provide researchers with a valuable
tool to expedite the development of new materials.